Ebook HPLC for Pharmaceutical Scientists, by Yuri V. Kazakevich, Rosario LoBrutto
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HPLC for Pharmaceutical Scientists, by Yuri V. Kazakevich, Rosario LoBrutto
Ebook HPLC for Pharmaceutical Scientists, by Yuri V. Kazakevich, Rosario LoBrutto
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HPLC for Pharmaceutical Scientists is an excellent book for both novice and experienced pharmaceutical chemists who regularly use HPLC as an analytical tool to solve challenging problems in the pharmaceutical industry. It provides a unified approach to HPLC with an equal and balanced treatment of the theory and practice of HPLC in the pharmaceutical industry.
In-depth discussion of retention processes, modern HPLC separation theory, properties of stationary phases and columns are well blended with the practical aspects of fast and effective method development and method validation. Practical and pragmatic approaches and actual examples of effective development of selective and rugged HPLC methods from a physico-chemical point of view are provided.
This book elucidates the role of HPLC throughout the entire drug development process from drug candidate inception to marketed drug product and gives detailed specifics of HPLC application in each stage of drug development.
The latest advancements and trends in hyphenated and specialized HPLC techniques (LC-MS, LC-NMR, Preparative HPLC, High temperature HPLC, high pressure liquid chromatography) are also discussed.
- Sales Rank: #2198495 in Books
- Published on: 2007-02-06
- Original language: English
- Number of items: 1
- Dimensions: 9.50" h x 2.30" w x 6.40" l, 3.82 pounds
- Binding: Hardcover
- 1140 pages
Review
"Without question LC/MS is the most dominant application of mass spectrometry in the pharmaceutical industry ... That being said, the editors should be commended for how well they took on such a comprehensive subject and worked with several recognized contributors to make a text that is both manageable and highly informative." (J Am Soc Mass Spectrom, 2007)
"...extremely useful and quite extensive in its coverage of the subject..." (Journal of the American Chemical Society, July 18, 2007)
From the Back Cover
Comprehensive coverage of modern HPLC theory, methodologies, and applications
This guide is a valuable resource for both novice and experienced pharmaceutical chemists who regularly use HPLC as an analytical tool to solve challenging problems in the pharmaceutical industry. A unified approach to HPLC with an equal and balanced treatment of the theory and practice of HPLC in the pharmaceutical industry is provided throughout the book.
- In-depth discussions of retention processes, modern HPLC separation theory, and properties of stationary phases and columns are well blended with the practical aspects of fast and effective method development and method validation
- Practical and pragmatic approaches and numerous examples of effective development of selective and rugged HPLC methods from a physico-chemical point of view are given
- This book elucidates the role of HPLC throughout the entire drug development process, from drug candidate inception to marketed drug product, and gives detailed specifics of HPLC application at each stage of drug development
- The latest advancements and trends in hyphenated and specialized HPLC techniques (LC-MS—small molecules and proteins, LC-NMR, Preparative HPLC, High temperature HPLC, Chiral HPLC, and Fast LC) are discussed
Authoritative and up to date, HPLC for Pharmaceutical Scientists is an ideal reference for pharmaceutical researchers working with HPLC, as well as for graduate students in analytical chemistry/biochemistry and pharmaceutical analysis programs.
About the Author
Dr. YURI KAZAKEVICH is an Associate Professor of Analytical Chemistry at Seton Hall University with thirty years of experience in liquid chromatography. He has over fifteen years of academic research experience in Russia and fifteen years of research, teaching and consulting for major American pharmaceutical companies, which has resulted in numerous papers and four book chapters. The main focus of Dr. Kazakevich's research is in HPLC retention mechanisms and the description of the analyte migration through the column with an emphasis on the influence of adsorbent geometry and surface chemistry. Dr. Kazakevich is the author of Basic Liquid Chromatography, one of the oldest and most complete online instructional resources on HPLC.
Dr. ROSARIO LOBRUTTO has over thirteen years of experience in the pharmaceutical industry working both with drug substances and drug products. He is a Group Head in the Pharmaceutical and Analytical Development Department at Novartis Pharmaceuticals Corporation managing multiple early to late phase projects for both small drug molecules and proteins/peptides and is responsible for teaching in-house HPLC method development training. Dr. LoBrutto is the author of twenty research articles, fifty presentations, and five book chapters in different areas of analytical/physical chemistry and has served as an adjunct professor for seven years. Dr. LoBrutto's main research directions include HPLC retention mechanisms, the influence of mobile phase modifiers on analyte retention and chromatographic figures of merit, and method development strategies for small molecules and proteins/peptides.
Most helpful customer reviews
8 of 9 people found the following review helpful.
excellent book
By Leon
This book covers the fundamentals of HPLC separation with the inclusion of most recent advancements in the areas, such as column technologies, UPLC and LC-NMR. I found this book is really useful in a sense it provides overviews in almost every stages in the drug industry from discovery and process development to formulation, drug metabolism, and commercialization. This directly helps me to work more effectively with analytical chemists from other functional areas. The authors surely understand what are the practical challenges that a bench analytical chemist is facing everyday and provide a lot of usful strategies such as method development recipe in chapter 8 to tackle the problems. Overview, I view this book as a great reference for HPLC separation and problem solving manual for the analytical chemists in pharmaceutical industry.
2 of 3 people found the following review helpful.
Nice for a little light reading :)
By L. Klungseth
This book is very in-depth.
It takes you from the fundamentals (what is the difference between reverse and normal phase HPLC?) to the small details (how will A2 values affect your separations?).
Some of the chapters were written by non-native English speakers, so some of the commas and other minor details are missing. This does not affect the quality of the information presented, it just means that sometimes you'll need to read a sentence twice in order to understand it.
This is a good read for both grad students and those working in industry.
0 of 0 people found the following review helpful.
Five Stars
By Izabella Khanoukova
I love it!
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